Studies toward the synthesis of azadirachtin, part 2 : construction of fully functionalized ABCD ring frameworks and unusual intramolecular reactions induced by close-proximity effects

Nicolaou, K. C., Sasmal, Pradip K., Koftis, Theocharis V., Converso, Antonella, Loizidou, Erika ORCID: https://orcid.org/0000-0002-4834-6639, Kaiser, Florian, Roecker, A. J., Dellios, Constantinos C., Sun, Xiao-Wen and Petrovic, Goran (2005) Studies toward the synthesis of azadirachtin, part 2 : construction of fully functionalized ABCD ring frameworks and unusual intramolecular reactions induced by close-proximity effects. Angewandte Chemie International Edition, 44 (22) . pp. 3447-3452. ISSN 1433-7851 [Article] (doi:10.1002/anie.200500217)

Abstract

The remarkable antifeedant agent and insecticide, azadirachtin (1), has, to date, escaped a total synthesis. The preparation of an advanced precursor has revealed some of the inner intricacies of this uniquely crowded and highly functionalized molecular architecture.

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